Synthesis and crystal structure determination of hydantoin-l-proline

Gerzon E. Delgado; Luis E. Seijas; Asiloé J. Mora

doi:10.1007/s10870-012-0344-3

Synthesis and crystal structure determination of hydantoin-l-proline

Gerzon E. Delgado
, Luis E. Seijas
, Asiloé J. Mora

Research output: Contribution to Journal › Research Article › peer-review

15 Scopus citations

Abstract

The title compound, hydantoin-l-proline, C ₆H ₈N ₂O ₂, crystallize in the orthorhombic system with space group P2 ₁2 ₁2 ₁ (N°19), Z = 4, and unit cell parameters a = 7.136(1) Å, b = 8.009(2) Å, c = 11.378(2) Å. The molecular structure shows a hydantoin and pyrrolidine ring coupling forming a bicyclohydantoin. The crystal packing is governed by N-H•••O hydrogen bond-type intermolecular interactions, forming infinite one-dimensional chains.

Original language	English (US)
Pages (from-to)	968-971
Number of pages	4
Journal	Journal of Chemical Crystallography
Volume	42
Issue number	9
DOIs	https://doi.org/10.1007/s10870-012-0344-3
State	Published - Sep 2012
Externally published	Yes

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This output contributes to the following UN Sustainable Development Goals (SDGs)

SDG 1 No Poverty

All Science Journal Classification (ASJC) codes

General Chemistry
Condensed Matter Physics

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10.1007/s10870-012-0344-3

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@article{c3933c6258314968ba77d00263194c7a,

title = "Synthesis and crystal structure determination of hydantoin-l-proline",

abstract = "The title compound, hydantoin-l-proline, C 6H 8N 2O 2, crystallize in the orthorhombic system with space group P2 12 12 1 (N°19), Z = 4, and unit cell parameters a = 7.136(1) {\AA}, b = 8.009(2) {\AA}, c = 11.378(2) {\AA}. The molecular structure shows a hydantoin and pyrrolidine ring coupling forming a bicyclohydantoin. The crystal packing is governed by N-H•••O hydrogen bond-type intermolecular interactions, forming infinite one-dimensional chains.",

author = "Delgado, \{Gerzon E.\} and Seijas, \{Luis E.\} and Mora, \{Asilo{\'e} J.\}",

note = "Funding Information: Acknowledgments This work was supported by CDCHT-ULA (Grant C-1755-11-08-B) and FONACIT (Grant LAB-97000821). The authors also thank to MSc. Teresa Gonz{\'a}lez and Dr. A. Brice{\~n}o, IVIC, Venezuela, for data collection.",

year = "2012",

month = sep,

doi = "10.1007/s10870-012-0344-3",

language = "English (US)",

volume = "42",

pages = "968--971",

number = "9",

}

TY - JOUR

T1 - Synthesis and crystal structure determination of hydantoin-l-proline

AU - Delgado, Gerzon E.

AU - Seijas, Luis E.

AU - Mora, Asiloé J.

N1 - Funding Information: Acknowledgments This work was supported by CDCHT-ULA (Grant C-1755-11-08-B) and FONACIT (Grant LAB-97000821). The authors also thank to MSc. Teresa González and Dr. A. Briceño, IVIC, Venezuela, for data collection.

PY - 2012/9

Y1 - 2012/9

N2 - The title compound, hydantoin-l-proline, C 6H 8N 2O 2, crystallize in the orthorhombic system with space group P2 12 12 1 (N°19), Z = 4, and unit cell parameters a = 7.136(1) Å, b = 8.009(2) Å, c = 11.378(2) Å. The molecular structure shows a hydantoin and pyrrolidine ring coupling forming a bicyclohydantoin. The crystal packing is governed by N-H•••O hydrogen bond-type intermolecular interactions, forming infinite one-dimensional chains.

AB - The title compound, hydantoin-l-proline, C 6H 8N 2O 2, crystallize in the orthorhombic system with space group P2 12 12 1 (N°19), Z = 4, and unit cell parameters a = 7.136(1) Å, b = 8.009(2) Å, c = 11.378(2) Å. The molecular structure shows a hydantoin and pyrrolidine ring coupling forming a bicyclohydantoin. The crystal packing is governed by N-H•••O hydrogen bond-type intermolecular interactions, forming infinite one-dimensional chains.

UR - https://www.scopus.com/pages/publications/84865517263

UR - https://www.scopus.com/pages/publications/84865517263#tab=citedBy

U2 - 10.1007/s10870-012-0344-3

DO - 10.1007/s10870-012-0344-3

M3 - Research Article

AN - SCOPUS:84865517263

SN - 1074-1542

VL - 42

SP - 968

EP - 971

JO - Journal of Chemical Crystallography

JF - Journal of Chemical Crystallography

IS - 9

ER -

Synthesis and crystal structure determination of hydantoin-l-proline

Abstract

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